DIGITAL LIBRARY
JUDUL | : | SINTESIS NITROSELULOSA DARI SELULOSA MURNI MENGGUNAKAN METODE NITRASI DENGAN ASAM SULFAT SEBAGAI KATALIS | |
PENGARANG | : | F ITRIANNOOR | |
PENERBIT | : | UNIVERSITAS LAMBUNG MANGKURAT | |
TANGGAL | : | 2020-11-27 |
Synthesis of nitrocellulose from pure cellulose using nitration method with
sulfuric acid as a catalyst had been done. The purpose of this research are to find a
characteristic of nitrocellulose and FT-IR absorbance. Nitrocellulose was
synthesized using nitration method in a mixture nitric acid, sulfuric acid and water
then cooled at 5OC - 15OC for 60 minutes. Results of research is showed that
nitrocellulose synthesized has a white solid form with acidity (flushing water) is
(pH) 7, water content is 7,77%, and Yield value is 84,15%. FT-IR character that
the formation nitro functional group (-NO2) sharp peak at 1635 cm-1 were
subtituted completely. However peak at 1361 cm-1 and 1288 cm-1 nitro functional
group (-NO2) incompletely substituted because peak outcome is not sharp. So two
hydroxyl functional group peak (-OH) at 3201 cm-1 and 3424 cm-1. Concluded,
substitution degree using absorbance ratio from FT-IR spectrum is 2,89.
Keyword : Nitrocellulose, pH, pure cellulose, Yield
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